Metals

At the RMS Foundation we can offer you the following services in the area of metal testing:

Please also note the following services from other categories

Corrosion measurements with EC-Pen

Description: The local measurement of the EC pen allows corrosion measurements (potentiodynamic measurements) to be carried out on real surfaces and thus, for example, the corrosion resistance of laser markings and markings can be compared with that of the base material. Pen tip: A = 1.5 mm2.
Standard(s):
  • Based on:
  • ISO 10993-15
  • ASTM G5
Newsletter: -
Equipment: EC-Pen with PGU Touch potentiostat

Contact:  Dieter Streit +41 32 644-2021

 

 

Composition of metals/alloys

Description:

Determination of the elemental composition of metals and alloys.

Standard(s):

various
Newsletter:
  • Chemical analysis by ICP-MS (NL-27)
  • Determination of the cleanliness of medical devices (NL-31)
Equipment:

X-ray Fluorescence (XRF) / Spark Optical Emission Spectroscopy (spark-OES) / Mass Spectrometry (ICP-MS)

 

 

Trace element analysis of metals and alloys

Description: Determination of trace elements in metals and alloys. Metal and alloy samples are digested in strong acid and required trace elements quantified by ICP-MS down to the ng/g range (DL are element-dependent). Alternatively, larger samples can be analyzed directly by spark-OES without digestion.
Standards(s):  
Newsletter:
  • Chemical analysis by ICP-MS (NL-27)
  • Determination of the cleanliness of medical devices (NL-31)
Equipment:

Mass spectrometry (ICP-MS) / Alternative: see Spark optical emission spektroscopy (spark-OES)

 

 

Sample preparation for materialographic examinations

Description: Preparation of specimens for materialographic studies such as cutting, embedding, grinding, polishing, and etching.
Standard(s):  
Newsletter:  
Equipment: Embedding press Metkon ECOPRESS®200 / Struers CitoPress / Grinding and polishing equipment Struers TegraPol-21 (+ Tegra Doser 5) and PRESI Meccatech 334

 

Contact:  Moritz Liesegang +41 32 644-2003

 

 

Determination of grain size, microstructure and volume fraction in multiphase microstructures

Description: Determination of the grain size index and the grain size based on standard methods as well as the volume fraction in multiphase microstructures according to the point counting method on metallic and ceramic materials with image documentation.
Standard(s):
  • ISO 643
  • ISO 20160
  • ASTM E 112
  • ASTM E 562
  • ASTM E 930
  • ETTC-3 / ETTC-4 / ETTC-8
Newsletter:  
Equipment: Leica DMI 5000 M light microscope with Jenoptik Gryphax Naos camera and IMS image management system

Contact:  Moritz Liesegang +41 32 644-2003

 

 

Determination of non-metallic inclusions in metals

Description: Characterization and determination of non-metallic inclusions on unetched sections of metallic materials with image documentation.
Standard(s):
  • ISO 4967
  • ASTM E45
Newsletter:  
Equipment: Leica DMI 5000 M light microscope with Jenoptik Gryphax Naos camera and IMS image management system

Contact:  Moritz Liesegang +41 32 644-2003

 

 

Content determination of precipitated phases

Description: Determination of the content of precipitated phases such as delta ferrite, sigma phase and iron beta phase by means of comparative reference series with image documentation.
Standard(s):
  • Dietmar Lober: Informationen über Stahl für Metallografen – Richtreihen und Normen für die Untersuchung: MVR 001 / 002 / 003
Newsletter:  
Equipment: Leica DMI 5000 M light microscope with Jenoptik Gryphax Naos camera and IMS image management system

Contact:  Moritz Liesegang +41 32 644-2003

 

 

Intergranular corrosion test according to ASTM A262 Practice A and E

Description: Intergranular corrosion tests on austenitic steels. Practice A (rapid screening test) includes the test for classification of etching structures. Practice E (copper/copper sulfate test) includes the determination of the sensitivity for intergranular grain boundary attack.
Standard(s):
  • ASTM A262
Newsletter:  
Equipment: Practice A: Electropolishing and etching equipment Buehler PoliMat 2 / Practice E: Glass apparatus with re-circulating cooling system

Contact:  Moritz Liesegang +41 32 644-2003

 

 

Conductivity measurement on non-ferrous metals

Description: Fast, non-destructive and precise measurement of the electrical conductivity of non-ferrous metals and alloys at different measuring frequencies.
Standard(s):
  • DIN EN 2004-1
  • ASTM E1004
Newsletter:  
Equipment: Fischer Sigmascope SMP1

Contact:  Dieter Streit +41 32 644-2021

 

 

Carrier gas hot extraction (TGHE) analyses of C, S, H, N, O and Ar in metals

Description: Carrier gas hot extraction analysis in an inert or reactive gas atmosphere for the quantitative determination of the elements carbon, sulfur, hydrogen, nitrogen, oxygen and argon in metallic and non-metallic materials.
Standard(s):
  • ASTM E1019
  • ASTM E1447
  • ASTM E1409
  • ASTM E2575
  • ISO 4491-4
  • ISO 5842
  • ASTM E1941
  • DIN EN ISO 14284
Newsletter:  
Equipment: LECO CS 230 Carbon Sulfur Analyzer / Bruker G8 Galileo & Mass Spectrometer ESD 100

 

 

Corrosion test (static immersion test)

Description:

Incubation of test specimens for 7 days in a test solution under in vitro conditions corresponding to the oral cavity, according to ISO 10271:2020, paragraph 4.1. Subsequent examination of the solutions and test specimens for optical changes and quantification of the released metallic ions by inductively coupled plasma-mass spectrometry (ICP-MS).

Standard(s):
  • ISO 10271
Newsletter:  
Equipment: Agilent 7700x ICP-MS

 

 

Detection of free iron on stainless steels (Practice F: For ferritic and martensitic steels of the 400 series)

Description:

The samples are tightly wrapped in paper towels. Prior to wrapping the paper towels are soaked in distilled water. The wrapped samples are then put in a glass dish with a lid on top to prevent evaporation. After 60 minutes, the samples are dried in a dry box. The test is positive if rust is detected visually or under the light-optical microscope at a 20x magnification.

The term free iron means iron present on the surface of parts, including but not limited to iron contaminations, iron-tool marks, residual iron. salts from pickling solutions, iron dust, atmospheric exposure, iron deposits in welds, embedded iron and iron oxide.

 

  • Suitable for ferritic and martensitic steels of the 400 series.
  • Detection of free iron in stainless steel.
  • Verification of a correctly performed surface passivation.
Standard(s):
  • A967 / A967M-17
Newsletter: -
Equipment: -

 

 

Detection of free iron on stainless steels (Practice E: For austenitic steels of the 200 and 300 series)

Description:

The samples are placed in a glass vessel filled with test solution. After 30 seconds, the samples are placed in a beaker containing distilled water and then dried in a drybox. The test is positive when a dark blue discoloration (Turnbulls blue) is visible 30 s later by eye or under the light-optical microscope (20x magnification).

The term free iron means iron present on the surface of parts, including but not limited to iron contaminations, iron-tool marks, residual iron. salts from pickling solutions, iron dust, atmospheric exposure, iron deposits in welds, embedded iron and iron oxide.

 

  • Suitable for austenitic steels of the 200 and 300 series.
  • Verification of a correctly performed surface passivation.
Standard(s):
  • A967/A967M-17
Newsletter: -
Equipment: -

 

 

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